The rigaku miniflex ii can be used for a variety of applications. Turn on cooling water water chiller to the left of the miniflex, wait for two minutes. Thanks to david carnevale for help in demonstrating the procedure. Log into pc and start rigaku guidance software load your sample in the sample holder. Used rigaku miniflex ii benchtop xray diffractometer ebay. If you have received and are installing jade for windows, follow the installation instructions that are in the jade manual. Our new rigaku smartlab xrd university of california. The iacs short courses have drawn over 3,500 student enrollments. External view of the miniflex 960129a26 including optional construction figure 1. Rigaku miniflex 600 miniflex school of chemical sciences at. Log into pc and start rigaku guidance software load your. The software allows semiquantitative analysis of almost all sample types without standards and. Rigaku miniflex benchtop xrd xray diffractometer system.
Source standard copper anode sealed tube source with tungsten filament. Rigaku xrd xray 6 manuals ruh2r rotating anode msc. Perhaps its most novel feature is the new smartlab studio ii software, which provides the user with an intelligent user guidance expert system functionality that guides the operator through the intricacies of each experiment. Copies of the oac and the radiation safety procedures manual for radiation. Before sharing sensitive information, make sure youre on a federal government site. Details of purchase order of miniflex 600 desktop x. Since its inception in 1951, rigaku has been at the forefront of analytical and industrial instrumentation technology. This is a rigaku dmax 2200 with a generator, high voltage transformer, horizontal goniometer, and scintillation detector.
Installing the miniflex ma101 sensor to ensure compliance with the stated measurement tolerance, the sensor must be positioned as shown in fig. The rigaku miniflex 600 is a compact benchtop theta. It is for instance possible to investigate crystal structures applying the fundamental parameters approach in the topas software, nanostructures for fast and reliable saxs measurements, or microstructures crystallite size. The miniflex ii power off button black can then turned off. Select omega window, toggle move and enter a value of. Collection of intensities of a full set of planes in the crystal contains the complete structural information about the molecule.
Its modular design and automated flow bar user interface has revolutionized access to the. The xrdsystem in wilcox 2 is a rigaku rotating anode high brilliance ru200bh. Edxrf xrf elemental analysis applied rigaku technologies. Watercirculating pump watercooled xray tube v cable highvoltage generator xray generator figure 2. When introduced in 1973, the original miniflex benchtop xrd was about onetenth the size, and dramatically less expensive, than. Rigaku announces 6th generation miniflex benchtop xrd system. Its failsafe radiation enclosure ensures the safety of users operating the machine. It is the newest addition to miniflex series of benchtop xray diffraction analyzers from rigaku, which began with the introduction of the original miniflex system decades ago. Miniflex standard software instruction manual manual no.
June 09, 2014 1 rigaku miniflex 600 operation notes standby condition power and cooling water on haskris chiller. Miniflex is the worlds smallest in size and lightest in weight. Rigaku xrdsystem instruction manual v41903 the krishnan groupwilcox 2, university of washington contents. The exceptional pricetoperformance ratio of the miniflex ii benchtop xray diffractometer sets a new standard for companies, universities, and other research institutions looking to add xrd capabilities to. Pdxl is rigakus fullfunction powder diffraction analysis package. Download download rigaku xrd manual read online read online rigaku xrd manual rigaku smartlab manual rigaku, miniflex 600,pdf rigaku xrd software rigaku miniflex 600 price rigaku xrd smartlab rigaku miniflex 600 manual rigaku xrd price rigaku ultima iv manual rigaku. Operating at 600 watts xray tube, the miniflex 600 is twice as powerful as other benchtop models, enabling faster analysis and improved overall throughput. The software user guide is a part of rigaku instructions booklet. Philips pw 1840 xray diffractometer wpw 1840 controller, instruction manuals. The rigaku miniflex xrd is a compact system that can be transported from the laboratory to the field.
Xg on indicator lamp on and tube set to 20kv and 2. Rigaku miniflex is a fully featured, general purpose xray diffractometer. Rigaku ultima iv powder diffractometer operation summary 11292012 a. It worked well when it got regular service from rigaku. The original instrument, and its successor that was introduced in 1976, employed a. Home boise state center for materials characterization. If you are about to initiate a run on the rigaku microxray diffractometer, you have already discussed with george harlow, the nature of the sample to be tested, the probable mounting configuration and run parameters, to render the best result for your research needs. Pdf owner manuals and user guides are not affiliated with the products andor names mentioned in this site. We would like to show you a description here but the site wont allow us. Xray fluorescence xrf provides one of the simplest, most accurate and most economic analytical methods for the determination of elemental composition of many types of materials. Scan sample xrays goniometer counter data output angle control counting controller ecp personal computer block diagram including optional construction. Operating the rigaku dmaxrapid microdiffractometer. The iacs advanced instrumentation is open to all qualified users, whether from princeton or outside, for an hourly fee which varies according to the category of user for example, industrial users are charged a competitive rate in comparison to that billed for similar analysis conducted by commercial laboratories, while undergraduates are. Amounts shown in italicized text are for items listed in currency other than canadian dollars and are approximate conversions to canadian dollars based upon bloombergs conversion rates.
Includes the mini flex, lytoron modular cooling system mc54050 series and miniflex standard software. Rigaku micro 2020 micro 2020, windows ce micro 2020, windows xpvista rigaku micro 2020 for pc and mobile devices micro 2020, windows xpvista sdk support for 3rd party libaries available user only max battery life dependant upon environmental conditions and usage. The rigaku miniflex ii can be used for a variety of applications from diffraction pattern. Insert miniflex program setup disk 1 into the floppy disk drive. Btx ii benchtop system is a fast, low cost, small footprint, benchtop xrd for full phase id of major, minor and trace components and quick xrf scan of elements ca u. Rigaku miniflex benchtop xrd xray diffractometer system crystallography desktop. Brandon mercado, our xray crystallography specialist, takes you through the basic workings of the rigaku miniflex 600 powder. Used rigaku miniflex ii benchtop xray diffractometer. This is a complex, computercontrolled instrument that has a lot of different capabilities. The rigaku miniflex xray diffractometer xrd is historically significant in that it was the first commercial benchtop tabletop or desktop xray diffractometry instrument. Rigaku ultima iv powder diffractometer operation summary 11.
The benchtop powder xray instrument is set up to collect pxrd in reflection mode with a. It hasnt been turned on in the last 15 years or so. Lincoln electric miniflex operators manual pdf download. Weld fume control for use with machines having product numbers. Terra mobile xrd system is a portable xrd analyzer that provides full phase id of major, minor and trace components with a quick xrf scan of elements ca u. Rigaku xray the latest instrument in rigaku s zsx series, the zsx primus continues the tradition of delivering accurate results in a timely and seamless manner, with unsurpassed reliability, flexibility, and ease of use to meet any challenges in todays laboratory. Rigaku user manual uwmadison geology 2 centering 1. Rigaku xrdsystem instruction manual v41903 the krishnan. If you purchased your computer from rigaku, the rs232c port is com1. The xrdsystem in wilcox 2 is a rigaku rotating anode high brilliance ru 200bh.
Startup if xrd is already started, with xray tube on, skip to step 4. Rigaku smartlab is the newest and most novel highresolution xray diffractometer xrd available today. Rigaku ultima iv powder diffractometer operation summary. When introduced in 1973, the original miniflex was about onetenth the size, and dramatically less expensive, than conventional xray diffraction equipment of the period.
Center and focus the area for xray measurement on the cross. It has two xray source paths diverging and parallel beam, a variety of slits and columnators, a regular and two hightemperature heating stages, and a 2d, solidstate detector. The boise state center for materials characterization was established by the idaho state board of education in august 2006 to provide a stateoftheart characterization facility in order to attract more students into science and engineering careers, to improve science and engineering education at. It has an associated database that may be useful for phase identification in your spectra. The d2 phaser is a portable desktop xrd instrument for research and quality control. In addition, it has an inplane arm axis which rotates the counter around the axis perpendicular to the axis of 2 rotation. Austin, texas, usa is responsible for the engineering and production of rigaku edxrf products worldwide. Xwppfwhole powder pattern fittingrirreference intensity ratio. Jun 14, 2012 rigaku micromax007hf manual products and names mentioned are the property of their respective owners. Running at 300 watts xray tube, the new miniflex 300 does not require an external heat exchanger.
Details of purchase order of miniflex 600 desktop xray. It is computer controlled and fully capable of providing qualitative and quantitative analyses for unknown powder crystalline materials. The rigaku ultima iii is a versatile xray diffraction system equipped with a high precision horizontal sample stage and a cross beam optics system to permit either high resolution parallel beam with a motor controlled multilayer mirror or braggbrentano parafocusing beam geometries. Rigaku technology and expertise provide a number of unique solutions for these determinations. Over 700 industrial scientists from more than 100 companies have utilized instruments in the iac. This site consists of a compilation of public information available on. The following writeup with photographs will show the alignment procedure to be done on rigaku ultima iii powder xray diffractometer rupxrd once in couple of months. The three primary software packages needed for use with the rigaku system are. General information safety how to turn on the xrays how to turn off the xrays general guidelines on how to use the xrdsystem seattle 3303 peter blomqvist. This rigaku miniflex benchtop xrd is in excellent condition and works perfectly. Our efforts have helped lead these industrial partners to many innovations and new product developments.
References and further reading rigaku miniflex ii system manual available in rm. Center and focus the area for xray measurement on the cross section using x, y and z screws. Opened, these software packages can be identified on the menu bar at the bottom of. Miniflex brochure book 04 2005 open computing facility. Established in 2009 as the energy dispersive xray fluorescence center of excellence division of rigaku corporation, applied rigaku technologies, inc. Featuring rigakus famous scatter fp method, the software can auto. Rigaku smartlab introduction the rigaku smartlab is a multipurpose xrd which can switch between focusing braggbrentano, bb and parallel beam pb geometries. New sixth generation miniflex benchtop xray diffractometer is a.
This site consists of a compilation of public information available on the internet. Cu xray tube auto sampler libraries sample holders chiller cables manuals. Specifications are subject to change without notice. The rigaku miniflex is historically significant in that it was the first commercial benchtop tabletop xray diffraction instrument. The rigaku miniflex ii can be used for a variety of applications from diffraction pattern comparison of polycrystalline materials such as powder samples and metal plates to qualitative and quantitative analyses and quality management of raw materials and products.
70 385 1673 44 710 1034 639 1450 942 429 165 784 11 477 147 1509 1178 822 331 1044 895 449 926 184 1068 830 1039 498 314 1446 206 471 1498 515